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1974, 6, 57; P. CrabM, Ger. , 1974, 81, 25191); G. Manuel, G. Cauquy, and P. Mazerolles, Syn. React. Inorg. Metal-Org. , 1974,4, 143. '')' R. W. Hoffmann, W. Lilienblum, and B. Dittrich, Chem. , 1974, 107. 3395. 201 Halogenocarbenes formed in the thermal decomposition of polyhalogenomethanes at 500--650°C can be trapped by cyclopentene and cyclohexene. 202 The thermal decomposition of CCl,SiF, in the vapour phase at 140°C in the presence of olefins leads to high yields of the corresponding gem-dichlorocyclopropanes, and an almost quantitative breakdown of the silane into dichlorocarbene and ClSiF, is inferred.
Hail, jun. and P. S. Chem. , 1974, 587. ”’ M. H. Rosen and G. Bonet, J. Org. , 1974,39, 3805. 274 275 276 277 278 L. H. 3810949 (Chem. , 1974,81, 63761). a. Barthes and M. Chaigneau, Compt. , 1974,279, C, 1017. I. T. Jacobson, Chem. Srripta, 1974, 5,227. T. Gibson, J. Org. , 1974,39, 845. M. Christ1 and G. Bruntrup, Chem. , 1974,107,3908.
Diirr and F. Werndorff, Angew. Chem. Internat. , 1974, 13, 483. N. Shimizu and S. Nishida, J . Amer. Chem. , 1974,96, 6451. G. A. Nikiforov, B. D. Sviridov, and V. V. Ershov, Izvest. Akad. , Ser. , 1974, 373 (Chem. , 1974, 81, 37312). 30 0. ’77 Si Me The spirane (113) was obtained on refluxing the diazopyrroline (114; R = CH,Ph or Bu) with N-phenyl maleimide, but with ADE the heterocycle (115) was formed by Alphen rearrangement of the initially formed pyrazole a d d ~ c t . ’ 79 Other additions’ 8o of diazoalkanes to olefins are illustrated in Scheme 11.